List of Analytical Services and Prices

 
Section Test Method (CDN $)
Physical Properties Aniline Point ASTM D611 95
  Ash of coals/coke ASTM D5142 39
  Ash of Petroleum Products ASTM D482 95
  Ash sulfated ASTM D874 114
  Bromine Number (BN) ASTM D1159 127
  Bulk Density ASTM D4512 55
  Catalyst Steaming ASTM D4463 517
  Calorific Value ASTM D2015 152
  Capacity Moisture of Coals ASTM D1412 95
  Cetane number ASTM 613 411
  Cloud Point ASTM D2500 136
  Color ASTM D1500 86
  Copper Corrosion Test ASTM D130 92
  Dean-Stark Soxholet extraction (large-300g)   242
  Dean-Stark Soxholet extraction (small-50g)   121
  Density of petroleum liquids ASTM D 4052 47
  Density of solids ASTM D2638 120
  Density of viscous petroleum products ASTM D2320 127
  Diene Value (MAV) UOP 326-82 246
  Electrical Conductivity ASTM D1125 50
  Flash Point ASTM 93 119
  Freezing Point ASTM 2386 119
  Insolubles, Pentane ASTM D4055 114
  Insoluble, Hexane   114
  Insoluble, Heptane ASTM D3279 114
  Insolubles, THF   114
  Insolubles, Toluene ASTM D4072 114
  Metal Impregnation   275
  Mercaptan Sulfur in Condensate by GC   363
  Mercaptan Sulfur in Crudes (including D86)   317
  Mercaptan Sulfur in Distillates (up to 270°C) ASTM D3227 184
  Micro Activity Test (MAT) ASTM D5154 380
  Micro Carbon Residue (MCRT) ASTM D4530 110
  Moisture of coals, coke, catalysts etc. ASTM D5142 39
  Moisture of crude oil by KF titration ASTM D4377/D1744 101
  Molecular Weight of hydrocarbons by VPO ASTM D2503 182
  Molecular Weight by Freezing Point Depression   121
  Octane Number (Motor) ASTM D2700 339
  Octane Number (Research) ASTM D2699 339
  Penetration Point  ASTM D5 94 
  Pour Point  ASTM D97  119
  TGA : general    303 
  TGA-FTIR    495 
  Proximate Analysis of coals, coke, etc.  ASTM D5142  66 
  Refractive Index  ASTM D1218  51 
  Reid Vapor Pressure  ASTM D323  145 
  Salt in Crude Oil  ASTM D6470M  242 
  Shell Hot Filtration Test (SHFT)  Shell SHFT  204 
  Smoke Point  ASTM D1322  194 
  Softening Point   ASTM D36  94 
  Total Acid Number (TAN)  ASTM D664  95 
  Total Base Number (TBN)  ASTM D2896  114 
  Viscosity by Brookfield viscometer  ASTM D5018  95 
  Viscosity by capillary viscometer  ASTM D445  95 
  Volatile Matter of coals/coke, etc.  ASTM D 5142  39 
  Water and Sediments in Fuel by Centrifuge  ASTM D1796  95 
  Centrifugation (4 X 1 L)  Sorval RC-3C Centrifuge  150 
Stability P-Value    440 
  Wiehe Compatibility Test  Wiehe method  440 
  Fouling of Liquid Hydrocarbons  Alcor HLPS (Hot Liquid Process Simulator)  1200 
  Existent Gum in Fuel by Jet Evaporation  ASTM D381  143 
  Oxydation Stability of Gasoline (Induction Period Method)  ASTM D525  220 
  Oxydation Stability of Aviation Fuels (Potential Residue Method)  ASTM D873  275 
  Oxydation Stability of Distillate Fuel Oil (Accelerated Method)  ASTM D2274  402 
  Thermal Oxyd. Stability of Aviat. Turbine Fuels (JFTOT)  ASTM D3241  330 
  Distillate Fuel Storage Stability at 43°C  ASTM D4625  424 
  Octel 180 or 90, 150°C Accelerated Fuel Oil Stability Test  ASTM D6468  275 
Elemental CHN (Carbon, Hydrogen,Nitrogen)  ASTM D5291/(ASTM D5373)  114 
  Total Sulfur (by X-Ray Fluorescence)  ASTM D4294  89 
  Total Sulfur (by comb. and IR)  ASTM D1552/(ASTM D4239)  89 
  Trace Sulfur (by GC-SCD or GC-AED, 0.1-100 ppm)  ASTM D5623  275 
  Elemental Sulphur  GC-AED  303 
  Forms of Sulphur (for Coals)  ASTM D2492  220 
  Trace Nitrogen (by Chemiluminescence Detection)  ASTM D 4629  101 
  Loss on ignition    77 
  Metals by ICPAES or ICP-MS    202 
  {It includes:     
  sample preparation (grinding/mixing/dissolution)    88 
  elements detection by ICP or ICP/MS}    114 
  Chlorine in Crude Oil and Petroleum fractions    495 
  {It includes:     
  ASTM D86 Distillation,      
  Potentiometric Titration of Chloride}     
  Oxygen (by direct determination)    114 
Gas Chromatography  Simulated Distillation by GC    286 
  Material with bp RT-210°C  ASTM 3710  286 
  Material with bp 50-525°C  ASTM D2887  286 
  Material with bp 50-615°C (Extended SIMDIST)  ASTM D2887 Ext  286 
  Material with bp 50-735°C   ASTM D6352  418 
  Material with bp 50-735°C and Residue  ASTM D7169  418 
  Refinery Gas Analysis (gas bag)  Fast MTI MicroGC  127 
  Refinery Gas Analysis-on line (24 hours monitoring)  Fast MTI MicroGC  473 
Advanced Characterization Sulfur compounds distribution by boiling point (GC-SCD)    330 
  Sulfur compound speciation by GC-SCD    by quotation
  Nitrogen compounds distribution by boiling point (GC-NCD)    330 
  Hydrocarbon Types by Column Eluition Chromatography:     
  SARA (Asphaltene + Saturates + Aromatics + Polars)  ASTM D2007M/ASTM D2549M  528 
  Asphaltenes (C5 or C7)    127 
  SOAP (Sat, Olefins, Arom, Polars) by SPE (Solid Phase Extraction)    627 
  SAP (Sat, Arom, Polars) by SPE    385 
  Total Olefins by SPE    242 
  Olefins distributed by boiling point (Separation by SPE + Sim Dist)    605 
  Hydrocarbon Types by SFC ASTM D5186  229 
  Hydrocarbon Types by FIA  ASTM D1319  209 
  Aromatics by IP-391  ASTM D6591/IP-391  220 
  Hydrocarbon Types ( 204-540 C) by GC-MS (Olefins not included   737 
  {It includes:     
  ASTM D 2007M or SAP -( Sat+Arom+Polars)    385 
  GC-MS ASTM D 2786- Saturates 204-540C)    176 
  GC-MS ASTM D 3239- Aromatics 204-545C) }    176 
  Hydrocarbon Types ( 204-540 C) by GC-MS (Olefins included   979 
  {It includes:     
  SOAP by SPE-( Sat + Olefins + Arom + Polars)    627 
  GC-MS ASTM D 2786- Saturates 204-540C)    176 
  GC-MS ASTM D 3239- Aromatics 204-545C) }    176 
  Hydrocarbon Types by HPLC-ELSD (>350C) (Saturates, Mono, Di, Polyaromatics)   886 
  Hydrocarbon Types by GC-FIMS   by quotation 
  Naphthalenes by UV  ASTM D1840 174 
  Total Naphthenic Acids  SPE-IR  506 
  Hydrocarbon Types Distribution by Boiling Point (by GC-SIMDIS-MS) (Olefins not included   1436 
  {It includes:     
  ASTM D 2007M or SAP- Sat + Arom + Polars    385 
  GC-MS ASTM D 2786- Saturates 204-540C)    176 
  GC-MS ASTM D 3239- Aromatics 204-545C)    176 
  ASTM D 2887 SIM DIST of Saturates    286 
  ASTM D 2887 SIM DIST of Aromatics    286 
  Calculation}    127 
  Hydrocarbon Types Distribution by Boiling Point (by GC-SIMDIS-MS) (Olefins included   2019 
  {It includes:     
  SOAP by SPE- (Sat + Olefins + Arom + Polars)    627 
  GC-MS ASTM D 2786- Saturates 204-540C)    176 
  GC-MS ASTM D 3239- Aromatics 204-545C)    176 
  ASTM D 2887 SIM DIST of Saturates    286 
  ASTM D 2887 SIM DIST of Aromatics    286 
  ASTM D 2887 SIM DIST of Olefins    286 
  Calculation}    182 
  Hydrocarbon Types by GC-MS (Robinson Method   303 
  Detailed Hydrocarbon Analysis (DHA) by High Resolution GC (RT-204C) CAN/CGSB-3.0 No.14.3-M94  466 
  Hydrocarbon Types (RT-204C) by PIONA (Without prefractionator) ASTM D6839  424 
  Hydrocarbon Types (RT-525C) by PIONA
(With prefractionator)
  710 
  {It includes:     
  Piona    424 
  Sim Dist}    286 
  H/C Ratio by GC-AED    by quotation 
  {It includes:      
  GC-AED run     
  Total CH by Leco or PE Analyzer}     
  GC-MS Analysis    
  Qualitative (Capillary GC+MS identification of major components)    253 
  Quantitative (SCAN or SIM with ISTD quantification of n compounds)    250+n*10 
Distillation  Distillation (atmospheric pressure)  ASTM D86  114 
  Distillation (vacuum, automatic, 200g charge)  ASTM D1160  595 
  Distillation (vacuum, manual, 200g charge, 5 fractions*)  ASTM D1160  595 
  Distillation (vacuum, manual, 500g charge, 5 fractions*)  ASTM D1160  727 
  Distillation (vacuum, manual, 1000g charge, 5 fractions*)  ASTM D1160  924 
  Distillation (vacuum, manual, 3000g charge, 5 fractions*)  ASTM D1160  1202 
  Small Spinning Band Distillation ( up to 3 L, up to 5 cuts, up to 350°C)    1200 
  Large Spinning Band Distillation ( up to 12 L, up to 5 cuts, up to 350°C)    2904 
  Distact     1200 
  TBP 15/5 Distillation (3 L)  ASTM D2892/D5236  2904 
  Dewatering for ASTM D2892/5236    660 
Surface characterization  Density of Solids by He Pycnometer  ASTM D2638 or D5550  120 
  Particle Size Distribution by Laser Granulometry  ASTM D4464/D197/C1070  120 
  Surface area (9 points) and Pore volume (1 point)  N2 adsorption  250 
  Surface area (9 points) and pore size distribution (24 point adsorption)  N2 adsorption  400 
  Surface area (9 points) and pore size distribution (up to 65 adsorption/desorption points)  N2 adsorption/desorption  460 
  Micropore Analysis    480 
  Chemisorption Analysis ( H2, CO, O2, H2S, CH4)    500 
  Temperature Programmed Reduction (TPR)    250 
  Temperature Programmed Desorption (TPD)    250 
  Temperature Programmed Oxidation (TPO)    250 
  Sequential TPR-TPD    300 
NMR Spectroscopy 13C Aromaticity    202 
  13C Spectrum    202 
  1H Spectrum    80 
  Olefin content by 1H NMR    140 
  Specialized NMR Services  2-D Experiments, carbon chemical functional group fingerprinting', etc  by quotation 

If the test you are looking for is not listed, please contact us. CanmetENERGY will accomodate special requests to meet clients needs.